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hplc instrument gilson 156 uv detector  (Gilson Inc)


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    Gilson Inc hplc instrument gilson 156 uv detector
    Hplc Instrument Gilson 156 Uv Detector, supplied by Gilson Inc, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/hplc+instrument+gilson+156+uv+detector/hplc+gilson/us12043607-5331-5-8
    Average 90 stars, based on 1 article reviews
    hplc instrument gilson 156 uv detector - by Bioz Stars, 2026-10
    90/100 stars

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    Residue:

    Article Title: HDAC inhibitors and therapeutic use thereof
    Article Snippet: The residue was purified by preparative HPLC (Instrument: Gilson GX-281 Liquid Handler, Gilson 322 Pump, Gilson 156 UV Detector; Column: 2_Phenomenex Gemini C18 75×40 mm×3 μm; Mobile phase A: H2O with 10 mmol NH4HCO3 (v %); Mobile phase B: MeCN; Gradient: B from 22% to 52% in 9.5 min, hold 100% B for 1 min; Flow Rate: 30 mL/min; Column Temperature: 30° C.; Wavelength: 220 nm, 254 nm) to afford N-[2-amino-5-[5-(1-hydroxyethyl)-2-thienyl]phenyl]-4-(methylsulfonimidoyl)benzamide (14.5 mg, 12.3% yield) as white solid.

    Purification:

    Article Title: HDAC inhibitors and therapeutic use thereof
    Article Snippet: The residue was purified by preparative HPLC (Instrument: Gilson GX-281 Liquid Handler, Gilson 322 Pump, Gilson 156 UV Detector; Column: 2_Phenomenex Gemini C18 75×40 mm×3 μm; Mobile phase A: H2O with 10 mmol NH4HCO3 (v %); Mobile phase B: MeCN; Gradient: B from 22% to 52% in 9.5 min, hold 100% B for 1 min; Flow Rate: 30 mL/min; Column Temperature: 30° C.; Wavelength: 220 nm, 254 nm) to afford N-[2-amino-5-[5-(1-hydroxyethyl)-2-thienyl]phenyl]-4-(methylsulfonimidoyl)benzamide (14.5 mg, 12.3% yield) as white solid.

    High Performance Liquid Chromatography:

    Article Title: HDAC inhibitors and therapeutic use thereof
    Article Snippet: The residue was purified by preparative HPLC (Instrument: Gilson GX-281 Liquid Handler, Gilson 322 Pump, Gilson 156 UV Detector; Column: 2_Phenomenex Gemini C18 75×40 mm×3 μm; Mobile phase A: H2O with 10 mmol NH4HCO3 (v %); Mobile phase B: MeCN; Gradient: B from 22% to 52% in 9.5 min, hold 100% B for 1 min; Flow Rate: 30 mL/min; Column Temperature: 30° C.; Wavelength: 220 nm, 254 nm) to afford N-[2-amino-5-[5-(1-hydroxyethyl)-2-thienyl]phenyl]-4-(methylsulfonimidoyl)benzamide (14.5 mg, 12.3% yield) as white solid.



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